{"id":6261,"date":"2022-07-26T08:19:05","date_gmt":"2022-07-26T00:19:05","guid":{"rendered":"https:\/\/www.xiaoxianmi.cn\/?p=6261"},"modified":"2022-10-12T10:13:05","modified_gmt":"2022-10-12T02:13:05","slug":"%e6%b0%af%e7%a2%b1%e7%9b%90%e6%b3%a5%e7%9a%84%e5%88%86%e6%9e%90","status":"publish","type":"post","link":"https:\/\/www.xiaoxianmi.cn\/en\/6261.html","title":{"rendered":"\u6c2f\u78b1\u76d0\u6ce5\u7684\u5206\u6790"},"content":{"rendered":"<p><strong><span style=\"font-size: 14pt;\">introductory<\/span><\/strong><\/p>\n<p>\u7126\u4f5c\u7164\u4e1a\uff08\u96c6\u56e2\uff09\u5f00\u5143\u5316\u5de5\u6709\u9650\u8d23\u4efb\u516c\u53f8\u5728\u79bb\u5b50\u819c\u6cd5\u5236\u78b1\u8fc7\u7a0b\u4e2d\uff0c\u4e3a\u4fdd\u8bc1\u7535\u89e3\u69fd\u9ad8\u6548\u7a33\u5b9a\u8fd0\u884c\uff0c\u5c06\u6de1\u76d0\u6c34\u3001\u78b1\u6027\u51b7\u51dd\u6c34\u3001\u6811\u8102\u518d\u751f\u5e9f\u6c34\u3001\u542b\u6c22\u5e9f\u6c34\u3001\u5de5\u4e1a\u6c34\u3001\u6ee4\u540e\u6db2\u7b49\u5404\u79cd\u6c34\u52a0\u5165\u914d\u6c34\u6876\u540e\uff0c\u91c7\u7528\u9006\u6d41\u63a5\u89e6\u5316\u76d0\uff0c\u83b7\u5f97\u4e86\u9971\u548c\u7684\u7c97\u76d0\u6c34\u3002\u8be5\u7c97\u76d0\u6c34\u7ecf\u8fc7\u524d\u53cd\u5e94\u6c60\u3001\u9884\u5904\u7406\u5668\u3001\u540e\u53cd\u5e94\u69fd\u3001HVM\u819c\u8fc7\u6ee4\u5668\u7b49\u591a\u79cd\u7cbe\u5236\u5de5\u5e8f\u540e\uff0c\u65b9\u53ef\u5411\u4e8c\u6b21\u76d0\u6c34\u53ca\u7535\u89e3\u5de5\u6bb5\u8f93\u9001\u5408\u683c\u7684\u9971\u548c\u7cbe\u76d0\u6c34\u3002\u901a\u5e38\u5411\u7c97\u76d0\u6c34\u4e2d\u52a0\u5165\u6c22\u6c27\u5316\u94a0\u3001\u78b3\u9178\u94a0\u3001\u4e09\u6c2f\u5316\u94c1\u7b49\u7cbe\u5236\u5242[1-2]\uff0c\u4e0e\u53ef\u6eb6\u6027\u6742\u8d28\u8fdb\u884c\u53cd\u5e94\u8f6c\u5316\u4e3a\u6eb6\u89e3\u5ea6 \u4f4e \u7684 \u6c89 \u6dc0 \u7269 \uff0c\u5206 \u522b \u7531 \u9884 \u5904 \u7406 \u5668 \u3001HVM\u819c \u8fc7 \u6ee4 \u5668 \u3001\u540e \u53cd \u5e94\u69fd\u6392\u51fa\uff0c\u8fd9\u4e9b\u6ce5\u6d46\u7ecf\u8fc7\u677f\u6846\u538b\u6ee4\u673a\u8131\u6c34\u3001\u6c34\u6d17\u3001\u98ce\u5e72\u5f97\u5230\u53ef\u8fd0\u8f93\u7684\u6c2f\u78b1\u76d0\u6ce5[3]\u3002\u8fd9\u79cd\u9884\u5904\u7406+HVM\u819c\u5de5\u827a\u6210\u719f\u53ef\u9760\u3001\u8fd0\u884c \u7a33 \u5b9a \uff0c\u4f46 \u56e0 \u76d0 \u6ce5 \u6210 \u5206 \u6742 \u3001\u542b \u76d0 \u91cf \u9ad8 \u3001\u9ecf \u5ea6 \u5927 \uff0c\u96be \u4ee5 \u5229 \u7528 \uff0c\u5916\u6392\u73af\u4fdd\u538b\u529b\u5927\uff0c\u4e0d\u5229\u4e8e\u4f01\u4e1a\u6e05\u6d01\u751f\u4ea7\u3002\u7126\u4f5c\u7164\u4e1a\uff08\u96c6\u56e2\uff09\u5f00\u5143\u5316\u5de5\u6709\u9650\u8d23\u4efb\u516c\u53f8\u7533\u62a5\u4e86\u201c\u6c2f\u78b1\u76d0\u6ce5\u56de\u6536\u5229\u7528\u5de5\u827a\u6280\u672f\u7814\u7a76\u201d\u6cb3\u5357\u80fd\u6e90\u7126\u7164\u96c6\u56e2\u7814\u53d1\u9879\u76ee\uff0c\u628a\u76d0\u6ce5\u56fa\u5e9f\u7684\u5904\u7406\u6446\u4e0a\u4e86\u8bae \u7a0b \uff0c\u8fd9 \u9700 \u8981 \u56de \u6536 \u76d0 \u6ce5 \u4e2d \u7684 \u76d0 \u5206 \uff0c\u964d \u4f4e \u539f \u76d0 \u6d88 \u8017 \uff1b\u5b9e \u73b0 \u8d44 \u6e90\u56de\u6536\u5229\u7528\uff0c\u51cf\u5c11\u5916\u6392\u76d0\u6ce5\uff0c\u4ece\u800c\u5b9e\u73b0\u6e05\u6d01\u751f\u4ea7\u3001\u53d1\u5c55\u5faa\u73af\u7ecf\u6d4e\u3001\u8282\u80fd\u51cf\u6392\u3002<\/p>\n<p>1 \u5b9e\u9a8c<\/p>\n<p>1.1 \u5b9e\u9a8c\u5668\u6750\u4eea\u5668\uff1a101\u578b \u7535 \u70ed \u9f13 \u98ce \u5e72 \u71e5 \u7bb1\uff08 \u4e2d \u5174 \u4f1f \u4e1a \uff09\uff0cBSA-224S-CW\u578b \u7535 \u5b50 \u5929 \u5e73\uff08 \u8d5b \u591a \u5229 \u65af \uff09\uff0cProflie plus\u578b\u7535\u611f\u8026\u5408\u7b49\u79bb\u5b50\u5149\u8c31\u4eea\uff08\u7f8e\u56fd\u5229\u66fc\uff09\uff0cUPHW-I-90T\u578b\u8d85\u7eaf\u6c34\u673a\u548c\u6c29\u6c14\u94a2\u74f6\uff08 \u8d85 \u7eaf \u79d1 \u6280 \uff09\uff0c70 mm\u00d735 mm\u7684\u4f4e\u578b\u79f0\u91cf\u74f6\u3002\u6750 \u6599 \uff1a\u6c2f \u78b1 \u76d0 \u6ce5 \u53d6 \u81ea2019\u5e741\u670821\u65e512\uff1a00\u5de6\u53f3\u672c\u516c\u53f8\u6c2f\u78b1\u5382\u4e00\u6b21\u76d0\u6c34\u5de5\u6bb5\u6392\u51fa\u7684\u672a\u98ce\u5e72\u76d0\u6ce5\uff1bpH\u8bd5 \u7eb8 \uff1b\u76d0 \u9178 \uff0c\u785d\u9178\u6c5e\uff0c\u785d\u9178\uff0c\u4e8c\u82ef\u57fa\u5076\u6c2e\u78b3\u9170\u80bc\uff0c\u6eb4\u767e\u91cc\u9999\u915a\u84dd\uff0c\u6309HG\/T 3696.3\u20142 011[4]\u3001GB\/T 601\u20142016[5]\u8981\u6c42\u914d\u5236\u8f85\u52a9\u8bd5\u5242\u548c\u6807\u6db2 \u3002\u9499\uff08Ca2+\uff09\u3001\u9541\uff08Mg2+\uff09\u3001\u94c1\uff08Fe3+\uff09\u3001\u94a1\uff08Ba2+\uff09\u3001\u94dd\uff08Al3+\uff09\u6807\u6db2\u8d28\u91cf\u6d53\u5ea6\u5747\u4e3a\uff1a1 000 \u03bcg\/mL\uff0c\u7845\uff08Si4+\uff09\u6807 \u6db2 \uff1a500 \u03bcg\/mL\uff1b\u5236\u5907Ca2+\u3001Mg2+\u3001Ba2+\u3001Fe3+\u3001Al3+\u3001Si4+\u6df7\u5408\u6807\u6db2\uff1a\u8981\u6c42Ca2+\u3001Mg2+\u8d28\u91cf\u6d53\u5ea6\u4e3a500 \u03bcg\/mL\uff0cFe3+\u3001Ba2+\u3001Al3+\u3001Si4+\u8d28\u91cf\u6d53\u5ea6\u4e3a10 \u03bcg\/mL\uff1b\u8d85 \u7eaf \u6c34 \u3002<\/p>\n<p>1.2 \u5b9e\u9a8c\u539f\u7406<\/p>\n<p>1.2.1 \u91cd\u91cf\u6cd5\u91c7\u7528\u6c14\u5316\u6cd5\u5c06\u88ab\u6d4b\u7ec4\u5206\u4ece\u8bd5\u6837\u4e2d\u5206\u79bb\u51fa\u6765\uff0c\u7ecf\u8fc7\u7cbe\u786e\u79f0\u91cf\u6765\u786e\u5b9a\u5f85\u6d4b\u7ec4\u5206\u542b\u91cf\u7684\u5206\u6790\u65b9\u6cd5\u3002<\/p>\n<p>1.2.2 \u6c5e\u91cf\u6cd5\u5728pH=2\uff5e3\u7684\u6eb6\u6db2\u4e2d\uff0c\u785d\u9178\u6c5e\u6807\u51c6\u6eb6\u6db2\u4e0e\u8bd5\u6837\u53cd\u5e94\uff0c\u5c06\u5f3a\u7535\u79bb\u7684\u785d\u9178\u6c5e\u8f6c\u5316\u4e3a\u5f31\u7535\u79bb\u7684\u6c2f\u5316\u6c5e\u3002\u6ef4\u5b9a\u7ec8\u70b9\u662f\u901a\u8fc7\u8fc7\u91cf\u785d\u9178\u6c5e\u4e0e\u4e8c\u82ef\u57fa\u5076\u6c2e\u78b3\u9170\u80bc\u6307\u793a\u5242\u53cd\u5e94\u751f\u6210\u7d2b\u7ea2\u8272\u5316\u5408\u7269\u6765\u6307\u793a\u3002<\/p>\n<p>1.2.3 \u7535\u611f\u8026\u5408\u7b49\u79bb\u5b50\u4f53\u539f\u5b50\u53d1\u5c04\u5149\u8c31\u6cd5\u672c\u7814\u7a76\u91c7\u7528\u7535\u611f\u8026\u5408\u7b49\u79bb\u5b50\u4f53\u539f\u5b50\u53d1\u5c04\u5149\u8c31\u6cd5\uff08Inductively Coupled Plasma-Atomic Emission Spectroscopy\uff0cICP-AES\uff09\uff0c\u5f85 \u6d4b \u6837 \u54c1 \u7531 \u9ad8 \u7eaf \u6c29 \u6c14 \u5f15 \u5165 \u96fe \u5316 \u7cfb\u7edf\u8fdb\u884c\u96fe\u5316\u540e\uff0c\u4ee5\u6c14\u4f53\u6eb6\u80f6\u7684\u5f62\u5f0f\u8fdb\u5165\u7b49\u79bb\u5b50\u4f53\u7684\u8f74\u5411\u901a\u9053\uff0c\u5728\u9ad8\u6e29\u548c\u60f0\u6027\u6c29\u6c14\u6c14\u6c1b\u4e2d\u88ab\u5145\u5206\u84b8\u53d1\u3001\u539f\u5b50\u5316\u3001\u7535\u79bb\u548c\u6fc0\u53d1\uff0c\u53d1\u5c04\u51fa\u6240\u542b\u5f85\u6d4b\u5143\u7d20\u7684\u7279\u5f81\u8c31\u7ebf\u3002\u56e0\u6b64\uff0c\u8bd5\u6837\u7ecf\u8fc7\u7a00\u91ca \u7279 \u5b9a \u500d \u6570 \u5904 \u7406 \u540e \uff0c\u5c06 \u5176 \u5438 \u5165ICP\u70ac \u7ba1 \uff0c\u5728 \u7279 \u5b9a \u6ce2 \u957f \u5904 \uff0c\u5206 \u522b\u6d4b\u91cfCa2+\u3001Mg2+\u3001Ba2+\u3001Fe3+\u3001Al3+\u3001Si4+\u91d1\u5c5e\u79bb\u5b50\u7684\u53d1\u5c04\u5149\u8c31\u8c31\u7ebf\u5f3a\u5ea6\u3002\u6839\u636e\u7279\u5f81\u8c31\u7ebf\u7684\u5b58\u5728\u4e0e\u5426\u3001\u7279\u5f81\u8c31\u7ebf\u5f3a\u5ea6\uff0c\u540c\u65f6\u8fdb\u884c\u5b9a\u6027\u4e0e\u5b9a\u91cf\u5206\u6790\u3002<\/p>\n<p>1.3 \u64cd\u4f5c\u6b65\u9aa4<\/p>\n<p>1.3.1 \u6837\u54c1\u5904\u7406\u79f0\u53d60.186 0 g\u76d0 \u6ce5 \uff0c\u52a0c\uff08HCl\uff09=0.201 3 mol\/L\u76d0\u9178\u6807\u51c6\u6eb6\u6db250 mL\u6eb6\u89e3\uff0c\u9178\u5316\u540e\u7684\u5c11\u91cf\u767d\u8272\u4e0d\u6eb6\u7269\u5728\u52a0\u6c34\u7a00\u91ca\u5b9a\u5bb9\u81f31 L\u8fc7\u7a0b\u4e2d\u9010\u6e10\u6d88\u5931\u3002\u7a7a\u767d\u5bf9\u7167\uff1a\u5438\u53d6c\uff08HCl\uff09=0.201 3 mol\/L\u76d0\u9178\u6807\u51c6\u6eb6\u6db250 mL\uff0c\u52a0 \u7eaf \u6c34 \u7a00 \u91ca \u5b9a \u5bb9 \u81f31 L\u30021.3.2 \u6c34\u5206\u7684\u6d4b\u5b9a\u6309GB\/T 13025.3\u20142012[6]\u7684 \u89c4 \u5b9a \u8fdb \u884c\u3002\u79f0 \u53d610 g\u7c89\u788e\u81f32 mm\u4ee5\u4e0b\u7684\u76d0\u6ce5\u5747\u5300\u8bd5\u6837\uff0c\u653e\u5165\u5df2\u5728\uff08110\u00b11\uff09\u00b0C \u6052 \u91cd \u7684 \u4f4e \u578b \u79f0\u91cf\u74f6\u4e2d\uff0c\u659c\u5f00\u79f0\u91cf\u74f6\u76d6\u653e\u5165101\u578b \u7535 \u70ed \u9f13 \u98ce \u5e72 \u71e5 \u7bb1 \u5185 \uff0c\u9010 \u6e10 \u5347\u81f3\uff08110\u00b11\uff09\u00b0C\uff0c\u5728\u8be5\u6052\u5b9a\u6e29\u5ea6\u4e0b\u5e72\u71e52 h\u3002\u76d6 \u4e0a \u79f0 \u91cf \u74f6 \u76d6 \u51b7\u5374 \u81f3 \u5ba4 \u6e29 \u540e \u79f0 \u91cf \uff0c\u4ee5 \u540e \u6bcf \u6b21 \u5e72 \u71e51 h\u540e\u51b7\u5374\u81f3\u5ba4\u6e29\u518d\u79f0\u91cf\uff0c\u76f4\u81f3\u8fde\u7eed\u4e24\u6b21\u79f0\u91cf\u4e4b\u5dee\u4e0d\u8d85\u8fc70.000 5 g\uff0c\u89c6 \u4e3a \u6052 \u91cd \u3002<\/p>\n<p>1.3.4 \u91d1\u5c5e\u79bb\u5b50\u7684\u6d4b\u5b9a\u5728\u7f16\u53f7\u4e3a1#\u30012#\u30013#\u7684100 m L\u5bb9 \u91cf \u74f6 \u4e2d \uff0c\u5206 \u522b \u6ce8 \u5165 \u6837 \u54c1\u5904\u7406\u6db250 mL\uff0c\u518d\u5206\u522b\u52a0\u5165\u5236\u5907\u7684Ca2+\u3001Mg2+\u3001Ba2+\u3001Fe3+\u3001Al3+\u3001Si4+\u6df7\u5408\u6807\u6db20 mL\u30015 mL\u300110 m L\uff0c\u7528 \u6c34 \u7a00 \u91ca \u81f3 \u523b \u5ea6 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